Matériaux Energétiques

Energetic materials such as rocket propellants or pyrotechnics present this paradox of containing high heat amounts which need to be stabilized during long periods of time but quickly released on demand. Thermal analysis together with thermokinetics allow for the assessment of the long term stability of such substances, together with a better understanding of their decomposition schemes and amounts of gases evolved.

Screening
The first and most simple step requires an assessment of each raw material, intermediate or final product to determine its thermal stability within plant conditions. This will determine if further investigation is required, and is performed using a DSC or TSu specific screening tool.

SADT, Time to Maximum Rate and the full package of thermal hazards data can be precisely determined using powerful kinetics software. With a well designed experimental series and advanced kinetics you significantly reduce the number of analysis required, reducing countless time and resources performing complex experimentation.

Some International References

Brochure

Une ligne d'analyseurs thermiques innovante (-120 / 830°C) avec la technologie du capteur

Sensys bénéficie des qualités métrologiques uniques du capteur "3D-Sensor Inside" (précision, reproductibilité, sensibilité) et couvre une très large gamme de température, allant de -120 à 830°C.
Grâce à sa modularité, SENSYS s'utilise avec diverses configurations:
- SENSYS DSC
mode DSC horizontal / vertical
Haute pression (jusqu'à 500 bars)
- SENSYS Robot DSC
- SENSYS TG-DSC-EGA simultanés

SENSYS evo DSC

SENSYS evo TG-DSC

Calorimètre isotherme de mélange et de réaction (ambiante à 300°C)

C80

Doté du capteur exclusif "Calvet 3D Sensor Inside" de Setaram, le C80 est le calorimètre le plus puissant disponible à ce jour

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Microcalorimetry (- 40°C to 200°C)

µSC

Setaram introduces the NEW µSC microcalorimeter featuring the ‘3D Calvet Sensor’ with unmatched sensitivity in both isothermal and scanning modes plus multiple sample capacity with zero cross talk sensors.

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Calorimètre Isotherme Très Haute Sensibilité (ambiante à 200°C)

MS80

Doté du capteur exclusif "Calvet 3D-Sensor", le calorimètre MS80 est considéré comme le calorimètre le plus sensible, essentiellement utilisé en mode isotherme.

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Software for kinetic analysis and thermal safety

AKTS advanced kinetics software is a unique and highly powerful software for precise and accurate mathematical modeling of even the most complex decompositions.
Using just a few C80 or DSC runs a precise simulation of your chemistry can be developed and then further accurate and scalable data such as Time to Maximum Rate, SADT and impacts of PHI-Factor can be calculated and then verified using a single ARC (PhiTEC-1) analysis.
This software, in combination with one or more of the above systems can allow you to have a complete and comprehensive understanding of your chemical system, from shelf life, SADT and process scale up.

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Mastering High Pressure DSC & Microcalorimetry up to 1000 bars - 14,500 psi

HP Micro DSC

Setaram sells the Gas Hydrates technology UNDER IFP's LICENCE (French Petroleum Industry) PA WO 2006/129018 A2

DSC measurement under very high pressure is of major importance for materials investigation and processes, to study PVT properties, in different fields such as energy (Gas hydrates), food, polymers, process safety, etc.
SETARAM's latest innovation is the Ultra High Pressure Gas Panel that allows DSC and calorimetry measurements up to 1000 bar.

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Analyseur de conductivité thermique - plus de tests en moins de temps.

TCi

Le TCi de C-Therm Technologies Ltd mesure la conductivité thermique et se présente comme un équipement “tout en un” capable de tester des solides, des liquides, des poudres et des pâtes. Cette technique C-Therm Technologies se présente sous la forme d'un outil de laboratoire dont les options permettent de rentabiliser toute activité de Recherche et Développement et d'améliorer le Contrôle Qualité. Point fort supplémentaire, cette technologie peut être parfaitement intégrée en production afin d’améliorer les divers procédés utilisés.

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Calorimétrie adiabatique de réaction

PHITEC I

The PHI-TEC I is a computer controlled adiabatic calorimeter that can be used to determin the heat evolved and pressure developed during an uncontrolled exothermic runaway reaction. It enables the user to understand what may happen during a worst case scenario arising from mal-operation.

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Calorimétrie adiabatique

PHITEC II

The PHI-TEC system is a computer controlled adiabatic calorimeter designed to simulate the thermal behaviour of larger scale chemical reactors, especially when studying uncontrolled and run-away reactions.

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Application Documents

Decomposition of nitrocellulose + nitroglycerine with kinetic study by C80 + AKTS >>See all application documents

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